高黏弹冻胶颗粒化流动特征及剪切造粒机制研究
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    摘要:

    本文研究颗粒化过程中高黏弹冻胶的流动特征和剪切造粒机制,对冻胶分散体的工业化生产与应用具有重要意义。对高黏弹冻胶在剪切装置中的颗粒化过程进行模拟计算,分析颗粒化过程压力场、速度场和剪切率场变化,揭示颗粒化过程中的流动规律;研究不同配液比、剪切转速、剪切间距、错齿间距和布齿角度等剪切参数下的剪切造粒机制。研究结果表明,剪切装置内主要分为剪切率最大的剪切破碎区域和出现压力极小值的颗粒混合区域,通过单因素影响规律和正交实验模拟研究,明确了剪切参数对流场中压力、速度、剪切率的影响贡献程度。明确了低温低盐、中高温中高盐、高温高盐和超高温超高盐四类本体冻胶在颗粒化设备剪切过程中的黏度、粒径和微观结构变化,剪切过程存在剪切破碎、混合磨碎、颗粒均一等三个阶段。以高温高盐本体冻胶为例通过调整配液比(1:0~1:9)、剪切转速(1160rpm~2900rpm)、剪切间距(1mm~5mm)、错齿间距(1.5mm~3mm)和布齿角度(-6°~6°)可以实时调整冻胶分散体粒径。通过模拟和室内实验方法,研究不同剪切参数对冻胶分散体体系的影响,明确高黏弹冻胶颗粒化影响因素,为现场应用提供参考。

    Abstract:

    This study investigates the flow characteristics and shear granulation mechanisms of high-viscoelastic gels during the granulation process, which holds significant importance for the industrial production and application of dispersed particle gels. The granulation process of high-viscoelastic gels within shear devices is simulated to analyze changes in the pressure field, velocity field, and shear rate field, thereby revealing the flow patterns during granulation. The shear granulation mechanisms under various parameters such as liquid mixing ratios, shear rotation speeds, shear distances, staggered tooth distances, and tooth arrangement angles are also studied. The results indicate that the shear device can be primarily divided into two regions: a high shear rate fragmentation region and a particle mixing region with minimal pressure values. Through single-factor influence analysis and orthogonal experimental simulations, the contributions of shear parameters to pressure, velocity, and shear rate in the flow field were clarified. Four types of bulk gels—low temperature and low salinity, moderate temperature and moderate salinity, high temperature and high salinity, and ultra-high temperature and ultra-high salinity—are examined for their viscosity, particle size, and microstructure changes during the shear granulation process in granulation equipment. This process includes three stages: shear fragmentation, mixed grinding, and particle uniformity. Taking high temperature and high salinity bulk gels as an example, adjustments to the liquid mixing ratio (1:0~1:9), shear rotation speed (1160rpm~2900rpm), shear distance (1mm~5mm), staggered tooth distance (1.5mm~3mm), and tooth arrangement angle (-6°~6°) allow for real-time adjustment of the dispersed particle gel size. By employing simulation and laboratory experiments, the impact of different shear parameters on the dispersed particle gel system was studied, identifying influencing factors for the granulation of high-viscoelastic gels. This provides references for practical applications.

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  • 收稿日期:2025-02-28
  • 最后修改日期:2025-04-16
  • 录用日期:2025-05-19
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